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<p class="MsoNormal"><span style="font-family:"Arial",sans-serif">Just a reminder, there is a pre-lab for exp 5 (EQW).<span style="mso-spacerun:yes">
</span>It must be completed before<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif">lab or you don’t get credit for it.<span style="mso-spacerun:yes">
</span>You’ll find it at the same site you found the<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif">notebook exercise and pre-lab and data entry for exp 1 (SCM).<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif"><o:p> </o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">We have not gotten to the material that applies to exp 5. I want to make<br>
sure you can answer all the questions from just the lab manual.<span style="mso-spacerun:yes">
</span>Contact<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">me or your TA if you have questions.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
The majority of what you need to complete the pre-lab is contained in the<br>
lab manual for exp 5. You will need an understanding of formula weights, <br>
the "mole" and molar mass. These are covered in sections 3.3 and 3.4.<br>
For further reading on ionic equations, acids and bases, and neutralization<br>
reactions see sections 4.2 and 4.3. Dilution is in section 4.5. We will be<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">getting to some of this in lecture tomorrow, unfortunately too late for Thursday<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">labs. Solution stoichiometry and titrations are covered in section 4.6. You<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">should look at this material in the book.
<span style="mso-spacerun:yes"> </span>However, you should be able to get<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">what you need for the pre-lab from the lab manual.<br>
<br>
Before attempting the pre-lab you should read the Discussion section<br>
and review the calculations. Write the procedure so you have some<br>
idea where the numbers are coming from. You can watch the video in<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">the pre-lab w/o answering any questions and then get out of the pre-lab.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">It won’t even register as having been done. It will give you a better idea<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">of what's going on so the procedure makes sense. You will have to<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">rewatch it when you actually do the pre-lab.<span style="mso-spacerun:yes">
</span>The procedure MUST<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">be written in your own words in an outline form similar to my example<br>
on the last page of the syllabus (and found at a <a href="http://chemistry.osu.edu/%7Erzellmer/chem1250/lab/notebook_proc_1250.pdf">
link </a>on my class web<br>
page). Pay attention to the equations and the examples in the manual<br>
since the calculations you'll be doing are very similar. <br>
<br>
In Part A of the exp you'll be using something with an acronym of KHP.<br>
People often mistakenly think KHP is potassium hydrogen phosphorus. <br>
It is <b>NOT</b>. <b>KHP is an acronym for potassium hydrogen phthalate</b>,<br>
<b>KHC<sub>8</sub>H<sub>4</sub>O<sub>4</sub></b>. It is a salt consisting of K<sup>+</sup> and HC<sub>8</sub>H<sub>4</sub>O<sub>4</sub><sup>-</sup>. The latter<br>
is a weak monoprotic acid (hydrogen phthalate). This is discussed in<br>
the lab manual in the Discussion and Lab Procedure sections of the<br>
manual (pages 24-28).<br>
<br>
The link for the pre-lab is in the syllabus, on Carmen and my web page<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">so
<span style="mso-spacerun:yes"> </span>if the following doesn't seem to work from your e-mail you can find<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">it somewhere.
<br>
<br>
<a href="https://uglabs.cbc.osu.edu/1250/pre-postlabs.php">https://uglabs.cbc.osu.edu/1250/pre-postlabs.php</a>
<br>
<br>
This will take you directly to the main Chem 1250 pre and post-lab page.<br>
READ this page and the Terms and Conditions of Use at the top if you<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">didn't do it already. I've sent instructions for how to use this in a previous<br>
e-mail. Remember, if you start again for any reason you have to watch<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">the video again and answer all the questions again.<br>
<br>
Once you click on the pre-lab or data-entry links you'll get a new screen.<br>
There is an INSTRUCTIONS button in a red box toward the upper-left of<br>
the page. Click on it before you start. Pay attention to what it's telling you<br>
to do in terms of units, how to enter the numbers, etc. <br>
<br>
The pre-lab essentially consists of two parts. The first part starts with<br>
a video, which you need to watch all the way through (including the<br>
credits) or you will have points deducted. Just let it run until it stops on<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">it's own.<span style="mso-spacerun:yes">
</span>Don’t move on to the next question until it stops.<span style="mso-spacerun:yes">
</span>Then there is<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">a series of questions dealing with the discussion and procedure in the<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">manual and the video.
<br>
<br>
Below this part is the data-entry part of the pre-lab. You'll be given<br>
numbers similar to what you'll obtain in the actual experiment. You will<br>
then do the appropriate calculations and enter the numbers (make sure<br>
you have the correct sig. fig.). That's pretty much it. <br>
<br>
When you are finished and satisfied with your answers click on the Submit<br>
button at the bottom. The program will send you an e-mail if the pre-lab<br>
was submitted correctly. Also, the screen should refresh with your entries<br>
and results and score. If it doesn't, it didn't submit properly.<br>
<br>
Dr. Zellmer <o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif"><o:p> </o:p></span></p>
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