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<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-bidi-font-family:"Times New Roman"">Ignore the “NOT READY”.<span style="mso-spacerun:yes">
</span>That was a note to myself while I was preparing<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-bidi-font-family:"Times New Roman"">it and I forgot to remove it.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-bidi-font-family:"Times New Roman""><o:p> </o:p></span></p>
<div>
<div style="border:none;border-top:solid #E1E1E1 1.0pt;padding:3.0pt 0in 0in 0in">
<p class="MsoNormal"><b><span style="mso-fareast-font-family:"Times New Roman"">From:</span></b><span style="mso-fareast-font-family:"Times New Roman""> Zellmer, Robert <zellmer.1@osu.edu>
<br>
<b>Sent:</b> Saturday, January 22, 2022 2:09 PM<br>
<b>To:</b> cbc-chem1250@groups.asc.ohio-state.edu<br>
<b>Cc:</b> cbc-chem1250-ta@groups.asc.ohio-state.edu<br>
<b>Subject:</b> exp 1 - report, graphing, report questions, etc. - NOT READY<o:p></o:p></span></p>
</div>
</div>
<p class="MsoNormal"><o:p> </o:p></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">I've received several questions concerning exp 1 report so I decided to send<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">something to everyone. I know some of you have already done exp 1 but this<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">should still help. There's a few things I've already e-mailed out, particularly<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">about the notebook, but are included here again.<br>
<br>
1) There was no report for exp 0 (ZER). There are reports for all the remaining exps.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><o:p> </o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><span style="mso-spacerun:yes">
</span>Some of what’s below was in a previous e-mail.<span style="mso-spacerun:yes">
</span>You’ll find information about what<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><span style="mso-spacerun:yes">
</span>goes in a report in general in the manual (see the CAK example starting on page<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><span style="mso-spacerun:yes">
</span>“xiv”) and the following link,<br>
<br>
<a href="https://uglabs.cbc.osu.edu/"><b>OSU Chemistry Undergraduate Laboratory Server - Very useful</b></a><br>
<br>
There you will find a Chem 1250 link and once there you will find several useful links<br>
about lab skills, lab notebook and report. I do have links to the Notebook and Report<br>
pages at this site and my "Laboratory" link and below. There's also info about the<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><span style="mso-spacerun:yes">
</span>notebook and report in Appendices A and B of the manual.<br>
<br>
2) All the reports are FULL reports exp the ones for exp 7.<br>
<br>
If you want to know what a FULL report is, look at the following two links,<br>
<br>
<a href="https://uglabs.cbc.osu.edu/gc-labreport/"><b>Chem Lab Report - Departmental Guidelines for Writing a Lab Report</b></a><br>
<br>
<a href="https://www.asc.ohio-state.edu/zellmer.1/chem1250/lab/chem1250_sample_lab_report.pdf">
<b>Lab Report Format - My Lab Report Example (outline)</b></a><br>
<br>
The 2nd one is my summary of what it should look like with what should go into<br>
each section. It is a little more up to date in that for most labs there are no report<br>
questions to answer in the manual.<span style="mso-spacerun:yes"> </span>
Some reports have Discussion and<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><span style="mso-spacerun:yes">
</span>Conclusion sections and some have only questions you answer.<br>
<br>
</span><span style="font-family:"Arial",sans-serif">For exps 1-6, 12 and 23 there are report questions you are suppose to answer<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""> and
</span><span style="font-family:"Arial",sans-serif">include with the report. This is in lieu of a Discussion and Conclusion section.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif">There are report question templates in Carmen you can download to make this<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif"><span style="mso-spacerun:yes">
</span>process easier.<span style="mso-spacerun:yes"> </span>You can find a link for them in the main experiment module.</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
<br>
</span><span style="font-family:"Arial",sans-serif">For exp 7 you will just be handing in a cover page, a graph, some pages from the<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif">lab manual and a single sample calculation. This is explained at the "Laboratory"<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif">link and the TA will explain it in lab at that time. There is a template you MUST<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif">use for this.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif"><o:p> </o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif"><span style="mso-spacerun:yes">
</span>Other reports will have Discussion and Conclusion sections.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
a) The procedure section in the report is simply a bibliographic reference unless<br>
you made any changes. We do NOT want any details of the procedure in the<br>
report. Any changes you make should go in this section below the bibliographic<br>
reference. Also, <b>for exp 1</b>, since the way you used each type of glassware is<br>
important to the results you should have written this down in your notebook during<br>
lab and include it in this section (i.e. did you use a 5-mL pipet 4 times for the 20 mL<br>
or did you use a 10-mL pipet 2 times).<br>
<br>
4) Each week you must have your notebook prepared when you walk into lab.<br>
The TA will come around the lab in the first 10 minutes or so and check to<br>
see if you have the notebook prepared. If not, you can loose up to 6 pts<br>
depending on how much you have done.<br>
<br>
Any data you take in lab or anything you do related to the exp should go in<br>
the notebook. Do <b>NOT </b>write in the manual or on another sheet of paper or<br>
anywhere else (even if you intend to copy it over to the notebook later).<br>
You will lose points for doing so.<br>
<br>
Record values to the correct sig. fig. and include units. Use tables when possible.<br>
<br>
</span><span style="font-family:"Arial",sans-serif">Always in <b><span style="color:red">PEN</span></b>. Use BLACK or BLUE ink. If you make a mistake put a<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif;color:red">single line</span><span style="font-family:"Arial",sans-serif"> through it and write the correct data next to it. Do
<b>NOT</b> use whiteout,<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif">scribble over the mistake or erase it. Again, if using an iPad for the notebook<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif">treat it as if it's a physical notebook. This means write in the notebook and do<br>
</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman"">
</span><span style="font-family:"Arial",sans-serif">NOT erase mistakes. Do what was just explained as if you're using paper.</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
<br>
The TA will grade your notebook (worth 10 pts) and tell you how to improve it.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><o:p> </o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""> You submit it to Carmen before leaving lab.<span style="mso-spacerun:yes">
</span>There’s a module for doing this for<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><span style="mso-spacerun:yes">
</span>each exp.<span style="mso-spacerun:yes"> </span>Following the directions for file type and naming convention.<br>
<br>
5) Exp 1 report<br>
<br>
a) Write a full report.<br>
<br>
b) </span><span style="font-family:"Arial",sans-serif">Go to the "Helpful Tidbits" link on my class web page (not Carmen) and you will find
<br>
<span style="mso-spacerun:yes"> </span>a link for exp 1 which should help with the lab itself and the report.</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
<br>
<a href="https://www.asc.ohio-state.edu/zellmer.1/chem1250/faq/faq_1250.htm">
<b>Helpful Tidbits for 1250</b></a><br>
<br>
c) </span><span style="font-family:"Arial",sans-serif">You will be making 4 graphs, one for each piece of glassware using the data from<br>
<span style="mso-spacerun:yes"> </span>the table. That's pretty much all you need from the table for the graphs. You will be<br>
<span style="mso-spacerun:yes"> </span>comparing your density from the graphs to that obtained from the data in the table.<br>
<span style="mso-spacerun:yes"> </span><span style="mso-spacerun:yes"> </span>You'll be using them to answer some questions.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif"><o:p> </o:p></span></p>
<p class="MsoNormal"><span style="font-family:"Arial",sans-serif"><span style="mso-spacerun:yes">
</span>Graph mass (y) vs. volume (x). Make sure the graph occupies the whole piece of paper<br>
<span style="mso-spacerun:yes"> </span>and spread the data out (good use of the axis) so it takes up most of the space of the graph.<br>
<span style="mso-spacerun:yes"> </span>Don't make the labels and titles huge (14 point font for graph title, 12 point font for axes<br>
<span style="mso-spacerun:yes"> </span>tittles, 10 pt font for axes labels). I have examples of good graphs at the link below. The<br>
<span style="mso-spacerun:yes"> </span>first graph isn't the best example since it doesn't take up the full page because I had to<br>
<span style="mso-spacerun:yes"> </span>shrink it so I could write on it at the top and bottom. This graphs shows you choose points<br>
<span style="mso-spacerun:yes"> </span>from the best-fit line for use in your sample calculations for slope (not your actual data<br>
<span style="mso-spacerun:yes"> </span>points). The 2nd graph is a better example of what a graph should look like. It also shows<br>
<span style="mso-spacerun:yes"> </span>an example of when you have more than one set of data plotted. In that case you need<br>
<span style="mso-spacerun:yes"> </span>a legend and you can bring the legend inside the graph area to allow the graph to<br>
<span style="mso-spacerun:yes"> </span>spread out and occupy the whole page. You don't need a legend when there's only<br>
<span style="mso-spacerun:yes"> </span>one set of data plotted (as for each graph in exp 1) since your title should indicate what's<br>
<span style="mso-spacerun:yes"> </span>being plotted. For most of the graphs this semester you only need a few grid lines (except<br>
<span style="mso-spacerun:yes"> </span>for exp 6 graphs). Also, Excel's default orientation is Landscape and that generally is<br>
<span style="mso-spacerun:yes"> </span>the best for graphs. For exp 6 you'll see that Portrait mode is the proper orientation.</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
<br>
<a href="https://www.asc.ohio-state.edu/zellmer.1/sample_graphs.pdf"><b>Sample Graphs</b></a><br>
<br>
There's also a link you can use to help get you started with Excel if you've never<br>
used it before. It's a simple example for a density graph. This is similar to what you<br>
are doing in exp 1 but not exactly the same. Go to the following link and you will find<br>
this, along with other useful links.<br>
<br>
<a href="https://www.asc.ohio-state.edu/zellmer.1/excel/excel.htm"><b>Using MS Excel for Reports</b></a><br>
<br>
Many of my examples use an older version of Excel (Excel 2003). I have a link<br>
explaining the major differences between it and the newer versions. Again, click tabs,<br>
right-click, etc. and explore what it can do and where to find things. There are Excel<br>
tutorials and videos all over the web (YouTube, Microsoft's web site). If you aren't<br>
sure about how to do something after looking for help please ask me.<br>
<br>
d) </span><span style="font-family:"Arial",sans-serif">You will use the graphs to answer some of the report questions. What is the density<br>
<span style="mso-spacerun:yes"> </span>from the graph and how does it compare to the average from the table? How does<br>
<span style="mso-spacerun:yes"> </span>determinate and indeterminate error show up on the graph? What should the intercept<br>
<span style="mso-spacerun:yes"> </span>be and why might your intercept not agree with this theoretical value? Include all 4<br>
<span style="mso-spacerun:yes"> </span>graphs in the report. Remember, 1 graph per page. How do the results from your table<br>
<span style="mso-spacerun:yes"> </span>compare to the results from the graphs? Which produces better values for the density?</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
<br>
</span><span style="font-family:"Arial",sans-serif">e) The last question deals with error. You must understand what is inherent error and that<br>
<span style="mso-spacerun:yes"> </span>it is not human error. It is described on page 11 of the lab manual.</span><span style="font-family:"Arial",sans-serif;mso-fareast-font-family:"Times New Roman""><br>
<br>
I'm will be sending a follow-up e-mail with a few more specifics about exp 1 data and graphs.<br>
<br>
I hope this and my on-line help file address the majority of your questions. If not, ask.<br>
<br>
Dr. Zellmer <o:p></o:p></span></p>
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